Laboratoire de recherche Génie des Procédés Chromatographie en Phase Gazeuse Présenté par : Dr. Ladjel segni.

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Transcription de la présentation:

Laboratoire de recherche Génie des Procédés Chromatographie en Phase Gazeuse Présenté par : Dr. Ladjel segni

Laboratoire de recherche Génie des Procédés Détendeu r

Injecteur

TYPES D’INJECTEURS

Fused silica tubing d c  0.3 mm d f  1  m L = m

Détecteur TCD

Exemple de chromatogramme CPG

Programmed Temperature GC (PTGC ) Programmed temperature Temperature is increased during run Good retention and resolution for wide range of boiling points Low temperature Weakly retained components (low boiling points) resolved Strongly retained components (high boiling points) not eluted in desired time High temperature Strongly retained components eluted and detected Weakly retained components poorly resolved

Chromatogramme d’une huile essentielle

GC/MS

Peak 1 Peak 2